二十二碳酸-d43酸蜂蜜中地美硝唑質(zhì)控樣品20g水稻中微量元素質(zhì)控樣品；水稻中鈣、銅、鐵、鉀、鎂、錳、鈉、磷、鋅質(zhì)控樣品20g

十三烷酸-d25酸（葡萄泥）水果中氯氟氰菊酯、高效氯氟氰菊酯質(zhì)控樣品；（葡萄泥）水果中氯氟氰菊酯、三氟氯氰菊酯質(zhì)控樣品30g大米中鎳質(zhì)控樣品；大米粉中鎳質(zhì)控樣品...

1-溴代十六烷-d33(花生粕)飼料中汞質(zhì)控樣品；飼料中Hg質(zhì)控樣品30g（魚肉泥）魚肉中揮發(fā)性鹽基氮質(zhì)控樣品20g

正癸基-d21醇糙米粉中總砷、機(jī)砷質(zhì)控樣品20g菠菜粉中鎂（Mg）質(zhì)控樣品@30g

己酸-d3酸奶粉中鄰苯二甲酸二異壬酯質(zhì)控樣品20g水中鉻質(zhì)控樣品50ml

辛酸-d3酸（青菜泥）蔬菜中肟菌酯質(zhì)控樣品30g奶粉中鄰苯二甲酸二正辛酯質(zhì)控樣品20g

正庚基-d15醇凍干人尿中汞質(zhì)量控制樣品10*5ml牛奶中鈣質(zhì)控樣品30ml

1-溴代十六烷-d3魚肉中脂肪酸質(zhì)控樣品30g防曬劑中水楊酸乙基己酯質(zhì)控樣品20g

正十二烷基-d25醇化妝品中總砷、總汞、鎘、鉛、砷、汞、鉻、pH值、二噁烷質(zhì)控樣品30g白砂糖中不溶解雜質(zhì)質(zhì)控樣品30g

正己基-d13醇魚肉中十四碳酸甲酯質(zhì)控樣品20g肉腸中酸性橙2號(hào)質(zhì)控樣品、肉腸中酸性橙Ⅱ號(hào)質(zhì)控樣品20g

1?4-丁烷-d8-二胺2HCl罐頭魚中揮發(fā)性鹽基氮質(zhì)控樣品60g（葡萄酒）果酒中有機(jī)酸質(zhì)控樣品；（葡萄酒）果酒中檸檬酸、乳酸質(zhì)控樣品30ml

1-溴代癸-d25餅干中總二氧化硫質(zhì)控樣品30g大米粉中鉛、鎘質(zhì)控樣品30g

1-溴戊烷-d3（大豆油）食用油中總脂肪酸質(zhì)控樣品20ml綠茶中靛藍(lán)質(zhì)控樣品30g

正戊基-d11醇蜂蜜中高果糖淀粉糖漿質(zhì)控樣品20g辣椒粉中鎘質(zhì)控樣30g

1-溴代癸-d3飲料中酸性橙Ⅱ號(hào)質(zhì)控樣品30ml大豆粉中水分、灰分、蛋白質(zhì)質(zhì)控樣品30ml

1-溴代烷-d3豬肉中特布他林質(zhì)控樣品20g濾膜中鎳質(zhì)控樣品1套

4-氟甲苯-d3飲用水中六氯苯質(zhì)控樣品30ml小麥粉中鉛質(zhì)控樣品30g

戊酸-d9酸（牛肉泥）肉制品中氯丙那林質(zhì)控樣品20g菜豆中氯氟氰菊酯和高效氯氟氰菊酯質(zhì)控樣品20g

胸苷-d4生活飲用水中釩質(zhì)控樣品50ml茶葉中鎘質(zhì)控樣品30g

1-溴十八烷-d37茶葉中鋅質(zhì)控樣品30g橄欖油中過氧化值、酸度、茴香胺值、碘值質(zhì)控樣品100ml